THE DESIGN AND ANALYSIS OF EXPERIMENTS. By Oscar Kempthorne. New York, John Wiley and Sons, Inc., 1952. 631 pp. $8.50. This book by a teacher of statistics (as well as a consultant for \"experimenters\") is a comprehensive study of the philosophical background for the statistical design of experiment. It is necessary to have some facility with algebraic notation and manipulation to be able to use the volume intelligently. The problems are presented from the theoretical point of view, without such practical examples as would be helpful for those not acquainted with mathematics. The mathematical justification for the techniques is given. As a somewhat advanced treatment of the design and analysis of experiments, this volume will be interesting and helpful for many who approach statistics theoretically as well as practically. With emphasis on the \"why,\" and with description given broadly, the author relates the subject matter to the general theory of statistics and to the general problem of experimental inference. MARGARET J. ROBERTSON

The Design and Analysis of Experiments

http://www.ibmc.up.pt/projectos/FJMonteiro/Bonamidi%20Project/References%20Bonamidi/Denry%20-%20State%20of%20the%20art%20zirconia%20dental%20applications.pdf

State of the art of zirconia for dental applications

This study investigates the critical maximum undeformed equivalent chip thickness for ductile-brittle transition (DBhmax-e) of zirconia ceramics under different lubrication conditions. A DBhmax-e model is developed through geometry and kinematics analyses of ductile-mode grinding. Result shows that DBhmax-e decreases with increasing friction coefficient (μ). An experimental investigation is then conducted to validate the model and determine the effect of dry lubrication, minimum quantity lubrication (MQL), and nanoparticle jet minimum quantity lubrication (NJMQL) conditions on DBhmax-e. According to different formation mechanisms of debris, the grinding behavior of zirconia ceramics is categorized into elastic sliding friction, plastic removal, powder removal, and brittle removal. Grinding forces per unit undeformed chip thickness (Fn/h and Ft/h) are obtained. The lubrication condition affects the normal force and ultimately influences the resultant force on workpiece. In comparison with dry grinding (DBhmax-e = 0.8 μm), MQL and NJMQL grinding processes increase DBhmax-e by 0.99 and 1.79 μm respectively; this finding is similar to model result. The theoretical model is then assessed by different volume fractions of nanofluids under NJMQL condition with an average percentage error of less than 8.6%.

Maximum undeformed equivalent chip thickness for ductile-brittle transition of zirconia ceramics under different lubrication conditions

The clinical success of modern dental ceramics depends on an array of factors, ranging from initial physical properties of the material itself, to the fabrication and clinical procedures that inevitably damage these brittle materials, and the oral environment. Understanding the influence of these factors on clinical performance has engaged the dental, ceramics, and engineering communities alike. The objective of this review is to first summarize clinical, experimental, and analytic results reported in the recent literature. Additionally, it seeks to address how this new information adds insight into predictive test procedures and reveals challenges for future improvements.

Performance of Dental Ceramics Challenges for Improvements

Compared to conventional machining (CM), ultrasonic vibration-assisted machining (UVAM) with high-frequency and small-amplitude has exhibited good cutting performances for advanced materials. In recent years, advances in ultrasonic generator, ultrasonic transducer, and horn structures have led to the rapid progress in the development of UVAM. Following this trend, numerous new design requirements and theoretical concepts have been proposed and studied successively, however, very few studies have been conducted from a comprehensive perspective. To address this gap in the literature and understanding the development trend of UVAM, a critical overview of UVAM is presented in this study, covering different vibration-assisted machining styles, device architectures, and theoretical analysis. This overview covers the evolution of typical hardware systems used to achieve vibratory motions from the one-dimensional UVAM to three-dimensional UVAM, the discussion of cutting characteristics with periodic separation between the tools and workpiece and the analysis of processing properties. Challenges for UVAM include ultrasonic vibration systems with high power, large amplitude, and high efficiency, as well as theoretical research on the dynamics and cutting characteristics of UVAM. Consequently, based on the current limitations and challenges, device improvement and theoretical breakthrough play a significant role in future research on UVAM.

Review of ultrasonic vibration-assisted machining in advanced materials

This paper summarises the high speed grinding characteristics of engineering ceramics. The performance in high speed grinding was compared with that of conventional speed grinding. Normal and tangential grinding forces and Acoustic Emission (AE) energy were measured to characterise the material removal characteristics of five polycrystalline ceramics. It was found that the microstructure and properties of the ceramic materials have significant influence on the removal and formation of their ground surfaces. Experimental results also demonstrated that grinding-induced vibration and coolant supply in high speed grinding of engineering ceramics are critical factors for achieving a satisfactory grinding performance.

Grinding characteristics of engineering ceramics in high speed regime

Abrasive machining of porcelain and zirconia with a dental handpiece

This article is to review the published works related to the CAD/CAM and in vitro finishing of bioceramics in restorative dentistry over the last two decades. Bioceramics with a wide spectrum of glass–ceramics, reinforced porcelains, zirconias, aluminas, fiber-reinforced ceramic composites and multi-layered ceramic structures are firstly classified with two categories based on their machinabilities. The investigations on the restorative performance with respect to wear, fatigue and durability are then summarized. Next, the technological challenges in dental CAD/CAM processes for rapid generation of crowns, inlays/onlays and bridges are reviewed. Furthermore, the research on the clinically applied abrasive finishing of bioceramics for intraoral final adjustments using high speed dental handpieces and diamond burs is addressed. Finally, the critical research issues relating to manufacturing are highlighted as future research trends for better applications of dental bioceramics in restorations.

An overview of in vitro abrasive finishing & CAD/CAM of bioceramics in restorative dentistry

High speed grinding of silicon nitride with resin bond diamond wheels

The influence of microstructure on the ultraprecision grinding response of a series of cemented carbides for spherical mirrors was characterized by means of optical and laser interferometry, atomic force microscopy, scanning electron microscopy and X-ray diffraction. Surface roughness, form accuracy, grinding-induced residual stress and material removal behaviors were studied as a function of tungsten carbide (WC) grain size. In connection with the removal mechanisms in ultraprecision grinding, microindentations performed on each material showed similar deformation patterns, all in the plastic regime. The microstructure of WC-Co materials was found to have little influence on the nanometre surface roughness and submicron form accuracy. However, the X-ray stress measurements indicated that the microstructure of carbide materials had a significant influence on the grinding-induced residual stresses; i.e. an increase in grinding-induced residual compressive stress with an decrease in WC grain size. No grinding-induced cracks were observed in the ground cemented carbide surfaces. The material removal in ultraprecision grinding was considered to occur within the ductile regime. The formation of microgrooves and plastic flow regions via slip bands of WC grains along the cobalt binder without visible resultant microfracturing of WC grains were the dominant removal mechanisms.

Ling Yin

Papers

Grinding characteristics of engineering ceramics in high speed regime

Abrasive machining of porcelain and zirconia with a dental handpiece

An overview of in vitro abrasive finishing & CAD/CAM of bioceramics in restorative dentistry

High speed grinding of silicon nitride with resin bond diamond wheels

Influence of microstructure on ultraprecision grinding of cemented carbides