Journal ArticleDOI
Increasing rates of reaction: microwave-assisted organic synthesis for combinatorial chemistry.
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This article is published in ACS Combinatorial Science.The article was published on 2002-03-01. It has received 327 citations till now. The article focuses on the topics: Organic synthesis.read more
Citations
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Journal ArticleDOI
Controlled microwave heating in modern organic synthesis.
TL;DR: This Review highlights recent applications of controlled microwave heating in modern organic synthesis, and discusses some of the underlying phenomena and issues involved.
Journal ArticleDOI
Microwaves in organic synthesis. thermal and non-thermal microwave effects
TL;DR: An overview of the thermal effects and the current state of non-thermal microwave effects is presented in this critical review along with a view on how these phenomena can be effectively used in organic synthesis.
Journal ArticleDOI
Microwave assisted synthesis – a critical technology overview
TL;DR: In this paper, the authors present a review of microwave assisted synthesis and separation protocols and discuss parallel reactions and scale-up of microwave-assisted synthesized reactions and separations, which are illustrated through experiments.
Journal ArticleDOI
Non-conventional methodologies for transition-metal catalysed carbon–carbon coupling: a critical overview. Part 2: The Suzuki reaction
TL;DR: In this paper, the authors considered non-conventional conditions: alternative coupling partners, ligandless, solid support, scCO 2, ionic liquds, fluorous media, water, microwave, ultrasound, micelles, microreactors, ball mill.
Journal ArticleDOI
Controlled microwave heating in modern organic synthesis: highlights from the 2004–2008 literature
C. Oliver Kappe,Doris Dallinger +1 more
TL;DR: In this review, more than 220 published examples of microwave-assisted synthetic organic transformations from the 2004 to 2008 literature are discussed and more than 500 reaction schemes are presented in the Electronic Supplementary Material.
References
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Journal ArticleDOI
The use of microwave ovens for rapid organic synthesis
R. N. Gedye,Frank E. Smith,Kenneth Charles Westaway,Humera Ali,Lorraine Baldisera,Lena Laberge,John Rousell +6 more
TL;DR: In this paper, four different types of organic reactions have been studied and seven different organic compounds have been prepared, under pressure in a microwave oven, and considerable rate increases have been observed.
Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TL;DR: In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.
Journal ArticleDOI
Developments in Microwave-Assisted Organic Chemistry
TL;DR: The CSIRO continuous microwave reactor (CMR) and microwave batch reactor (MBR) were developed for organic synthesis and operated at temperatures up to 200°C (1400 kPa) and 260°C(10 MPa) respectively as discussed by the authors.
Journal ArticleDOI
Microwave activation in phase transfer catalysis
TL;DR: A review of the up-to-date experiments in phase transfer catalysis can be found in this article, with a focus on the solvent-free conditions of the phase transfer process and its application in organic synthesis.
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Microwave assisted organic synthesis-a review
A tentative rationalization of microwave effects in organic synthesis according to the reaction medium, and mechanistic considerations
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